NOAEL Studies Cosmetic Ingredient

m-Phenylenediamine NOAEL Studies

INCI: M-PHENYLENEDIAMINE

CAS: 108-45-2

Raw No Observed Adverse Effect Level endpoint records grouped by source. This page does not render calculated Margin of Safety values.

CIR_vision_codex 12 endpoints
Source Endpoint Type Value Unit Species Route Duration Study Type Reference
CIR_vision_codex NOAEL =6 mg/kg rat dermal Subchronic repeated dose toxicity {"citation":"2; 0; 6","dose":"Toxic effects were not observed in rats dosed with 2.0 or 6.0 mg/kg m-Phenylenediamine.","effect":"test substance-related effect could be made based on necropsy findings in animals that survived to the end of the study. Necropsy results included isolated evidence of various spontaneous alterations, such as congenital fissurations of the spleen and liver nodules or testicular atrophy. Toxic effects were not observed in rats dosed with 2.0 or 6.0 mg/kg m-Phenylenediamine. It was concluded that the highest daily dose that could be administered to a group without cumulative damage and/or substance-related changes (no-effect-level) was 6 mg m- Phenylenediamine/kg body weight. Subchronic Dermal Toxicity The subchronic dermal toxicity of an oxidative dye formulation contain- ing 1.5% m-Phenylenediamine was evaluated using 12 adult New Zealand white rabbits (six males, six females; weights not stated). Three groups of 12 untreated rabbits served as controls. The dye was mixed with an equal volume of 6% hydrogen peroxide and applied (dose = 1 mL/kg) to the dorsolateral aspects of the thoracic-lumbar area (one on each side of the midline). The test sites were alternated in order to minim...","page":18,"pdf":"PRS62.pdf","row_type":"noael_study","study_id":"PRS62_noael_001"}
CIR_vision_codex NOAEL =5 mg/kg rat - - developmental toxicity {"citation":"5; 7; (99","dose":"It was concluded that m-Phenylenediamine was not neurotoxic and that the no observable effect level for this chemical in male and female rats was 5 mg/kg (Du Pont, 1992).","effect":"ons were not considered neurotoxic effects but were considered indicative of general malaise in experimental animals. The general malaise was supported by concurrent clinical observations of lethargy. In female rats, the test substance did not induce changes in horizontal or vertical motor activity counts at any of the doses tested. Neuropathologic exam- inations did not indicate any abnormalities within the nervous system or skeletal muscle. It was concluded that m-Phenylenediamine was not neurotoxic and that the no observable effect level for this chemical in male and female rats was 5 mg/kg (Du Pont, 1992). Reproductive Toxicity The results of six reproductive toxicity studies are summarized in Table 7. In the first study, the fetal toxicity of m-Phenylenediamine (99% pure) in water was evaluated using 125 female rats (weights = 200-250 g) that had been mated for the first time. The test substance was administered orally to three groups of 25 rats in doses of 10, 30, and 90 mg/kg/day, respectively, on gestation days 5 to 16. The doses were administered once daily at a dose volu...","page":25,"pdf":"PRS62.pdf","row_type":"noael_study","study_id":"PRS62_noael_002"}
CIR_vision_codex NOAEL =134 mg/kg/day rat oral 2-week repeated dose toxicity {"citation":"250; 500; (3","dose":"ethal dose in a group of six rabbits was in the range of 250 mg/kg to 500 mg/kg.","effect":"ethal dose in a group of six rabbits was in the range of 250 mg/kg to 500 mg/kg. Minimal nephrosis was the only pathologic change noted in six rats dosed orally with m-Phenylenediamine (3% suspension in peanut oil; dose = 90 mg/kg/day) over a 2-week period. There were not test sub- stance-related pathologic changes in six rats dosed (intragastric intu- bation) with 0.8% m-Phenylenediamine (in mixture; 134 mg/kg/day) over a 2-week period. In a subchronic (90-day) oral toxicity study involving groups of 20 rats, the no-effect level was 6 mg m-Phenylenediamine/kg body weight. At histopathologic examination, degenerative lesions in the liver were observed only in the 18-mg/kg/day dose group. There was no indication of toxic injury to the kidneys.","page":48,"pdf":"PRS62.pdf","row_type":"noael_study","study_id":"PRS62_noael_003"}
CIR_vision_codex NOAEL =6 mg/kg rat dermal Subchronic repeated dose toxicity {"citation":"2; 0; 6","dose":"Toxic effects were not observed in rats dosed with 2.0 or 6.0 mg/kg m-Phenylenediamine.","effect":"test substance-related effect could be made based on necropsy findings in animals that survived to the end of the study. Necropsy results included isolated evidence of various spontaneous alterations, such as congenital fissurations of the spleen and liver nodules or testicular atrophy. Toxic effects were not observed in rats dosed with 2.0 or 6.0 mg/kg m-Phenylenediamine. It was concluded that the highest daily dose that could be administered to a group without cumulative damage and/or substance-related changes (no-effect-level) was 6 mg m- Phenylenediamine/kg body weight. Subchronic Dermal Toxicity The subchronic dermal toxicity of an oxidative dye formulation contain- ing 1.5% m-Phenylenediamine was evaluated using 12 adult New Zealand white rabbits (six males, six females; weights not stated). Three groups of 12 untreated rabbits served as controls. The dye was mixed with an equal volume of 6% hydrogen peroxide and applied (dose = 1 mL/kg) to the dorsolateral aspects of the thoracic-lumbar area (one on each side of the midline). The test sites were alternated in order to minim...","page":18,"pdf":"PRS62.pdf","row_type":"noael_study","study_id":"PRS62_noael_001"}
CIR_vision_codex NOAEL =5 mg/kg rat - - developmental toxicity {"citation":"5; 7; (99","dose":"It was concluded that m-Phenylenediamine was not neurotoxic and that the no observable effect level for this chemical in male and female rats was 5 mg/kg (Du Pont, 1992).","effect":"ons were not considered neurotoxic effects but were considered indicative of general malaise in experimental animals. The general malaise was supported by concurrent clinical observations of lethargy. In female rats, the test substance did not induce changes in horizontal or vertical motor activity counts at any of the doses tested. Neuropathologic exam- inations did not indicate any abnormalities within the nervous system or skeletal muscle. It was concluded that m-Phenylenediamine was not neurotoxic and that the no observable effect level for this chemical in male and female rats was 5 mg/kg (Du Pont, 1992). Reproductive Toxicity The results of six reproductive toxicity studies are summarized in Table 7. In the first study, the fetal toxicity of m-Phenylenediamine (99% pure) in water was evaluated using 125 female rats (weights = 200-250 g) that had been mated for the first time. The test substance was administered orally to three groups of 25 rats in doses of 10, 30, and 90 mg/kg/day, respectively, on gestation days 5 to 16. The doses were administered once daily at a dose volu...","page":25,"pdf":"PRS62.pdf","row_type":"noael_study","study_id":"PRS62_noael_002"}
CIR_vision_codex NOAEL =134 mg/kg/day rat oral 2-week repeated dose toxicity {"citation":"250; 500; (3","dose":"ethal dose in a group of six rabbits was in the range of 250 mg/kg to 500 mg/kg.","effect":"ethal dose in a group of six rabbits was in the range of 250 mg/kg to 500 mg/kg. Minimal nephrosis was the only pathologic change noted in six rats dosed orally with m-Phenylenediamine (3% suspension in peanut oil; dose = 90 mg/kg/day) over a 2-week period. There were not test sub- stance-related pathologic changes in six rats dosed (intragastric intu- bation) with 0.8% m-Phenylenediamine (in mixture; 134 mg/kg/day) over a 2-week period. In a subchronic (90-day) oral toxicity study involving groups of 20 rats, the no-effect level was 6 mg m-Phenylenediamine/kg body weight. At histopathologic examination, degenerative lesions in the liver were observed only in the 18-mg/kg/day dose group. There was no indication of toxic injury to the kidneys.","page":48,"pdf":"PRS62.pdf","row_type":"noael_study","study_id":"PRS62_noael_003"}
CIR_vision_codex NOAEL =6 mg/kg rat dermal Subchronic repeated dose toxicity {"citation":"2; 0; 6","dose":"Toxic effects were not observed in rats dosed with 2.0 or 6.0 mg/kg m-Phenylenediamine.","effect":"test substance-related effect could be made based on necropsy findings in animals that survived to the end of the study. Necropsy results included isolated evidence of various spontaneous alterations, such as congenital fissurations of the spleen and liver nodules or testicular atrophy. Toxic effects were not observed in rats dosed with 2.0 or 6.0 mg/kg m-Phenylenediamine. It was concluded that the highest daily dose that could be administered to a group without cumulative damage and/or substance-related changes (no-effect-level) was 6 mg m- Phenylenediamine/kg body weight. Subchronic Dermal Toxicity The subchronic dermal toxicity of an oxidative dye formulation contain- ing 1.5% m-Phenylenediamine was evaluated using 12 adult New Zealand white rabbits (six males, six females; weights not stated). Three groups of 12 untreated rabbits served as controls. The dye was mixed with an equal volume of 6% hydrogen peroxide and applied (dose = 1 mL/kg) to the dorsolateral aspects of the thoracic-lumbar area (one on each side of the midline). The test sites were alternated in order to minim...","page":18,"pdf":"PRS62.pdf","row_type":"noael_study","study_id":"PRS62_noael_001"}
CIR_vision_codex NOAEL =5 mg/kg rat - - developmental toxicity {"citation":"5; 7; (99","dose":"It was concluded that m-Phenylenediamine was not neurotoxic and that the no observable effect level for this chemical in male and female rats was 5 mg/kg (Du Pont, 1992).","effect":"ons were not considered neurotoxic effects but were considered indicative of general malaise in experimental animals. The general malaise was supported by concurrent clinical observations of lethargy. In female rats, the test substance did not induce changes in horizontal or vertical motor activity counts at any of the doses tested. Neuropathologic exam- inations did not indicate any abnormalities within the nervous system or skeletal muscle. It was concluded that m-Phenylenediamine was not neurotoxic and that the no observable effect level for this chemical in male and female rats was 5 mg/kg (Du Pont, 1992). Reproductive Toxicity The results of six reproductive toxicity studies are summarized in Table 7. In the first study, the fetal toxicity of m-Phenylenediamine (99% pure) in water was evaluated using 125 female rats (weights = 200-250 g) that had been mated for the first time. The test substance was administered orally to three groups of 25 rats in doses of 10, 30, and 90 mg/kg/day, respectively, on gestation days 5 to 16. The doses were administered once daily at a dose volu...","page":25,"pdf":"PRS62.pdf","row_type":"noael_study","study_id":"PRS62_noael_002"}
CIR_vision_codex NOAEL =134 mg/kg/day rat oral 2-week repeated dose toxicity {"citation":"250; 500; (3","dose":"ethal dose in a group of six rabbits was in the range of 250 mg/kg to 500 mg/kg.","effect":"ethal dose in a group of six rabbits was in the range of 250 mg/kg to 500 mg/kg. Minimal nephrosis was the only pathologic change noted in six rats dosed orally with m-Phenylenediamine (3% suspension in peanut oil; dose = 90 mg/kg/day) over a 2-week period. There were not test sub- stance-related pathologic changes in six rats dosed (intragastric intu- bation) with 0.8% m-Phenylenediamine (in mixture; 134 mg/kg/day) over a 2-week period. In a subchronic (90-day) oral toxicity study involving groups of 20 rats, the no-effect level was 6 mg m-Phenylenediamine/kg body weight. At histopathologic examination, degenerative lesions in the liver were observed only in the 18-mg/kg/day dose group. There was no indication of toxic injury to the kidneys.","page":48,"pdf":"PRS62.pdf","row_type":"noael_study","study_id":"PRS62_noael_003"}
CIR_vision_codex NOAEL =6 mg/kg rat dermal Subchronic repeated dose toxicity {"citation":"2; 0; 6","dose":"Toxic effects were not observed in rats dosed with 2.0 or 6.0 mg/kg m-Phenylenediamine.","effect":"test substance-related effect could be made based on necropsy findings in animals that survived to the end of the study. Necropsy results included isolated evidence of various spontaneous alterations, such as congenital fissurations of the spleen and liver nodules or testicular atrophy. Toxic effects were not observed in rats dosed with 2.0 or 6.0 mg/kg m-Phenylenediamine. It was concluded that the highest daily dose that could be administered to a group without cumulative damage and/or substance-related changes (no-effect-level) was 6 mg m- Phenylenediamine/kg body weight. Subchronic Dermal Toxicity The subchronic dermal toxicity of an oxidative dye formulation contain- ing 1.5% m-Phenylenediamine was evaluated using 12 adult New Zealand white rabbits (six males, six females; weights not stated). Three groups of 12 untreated rabbits served as controls. The dye was mixed with an equal volume of 6% hydrogen peroxide and applied (dose = 1 mL/kg) to the dorsolateral aspects of the thoracic-lumbar area (one on each side of the midline). The test sites were alternated in order to minim...","page":18,"pdf":"PRS62.pdf","row_type":"noael_study","study_id":"PRS62_noael_001"}
CIR_vision_codex NOAEL =5 mg/kg rat - - developmental toxicity {"citation":"5; 7; (99","dose":"It was concluded that m-Phenylenediamine was not neurotoxic and that the no observable effect level for this chemical in male and female rats was 5 mg/kg (Du Pont, 1992).","effect":"ons were not considered neurotoxic effects but were considered indicative of general malaise in experimental animals. The general malaise was supported by concurrent clinical observations of lethargy. In female rats, the test substance did not induce changes in horizontal or vertical motor activity counts at any of the doses tested. Neuropathologic exam- inations did not indicate any abnormalities within the nervous system or skeletal muscle. It was concluded that m-Phenylenediamine was not neurotoxic and that the no observable effect level for this chemical in male and female rats was 5 mg/kg (Du Pont, 1992). Reproductive Toxicity The results of six reproductive toxicity studies are summarized in Table 7. In the first study, the fetal toxicity of m-Phenylenediamine (99% pure) in water was evaluated using 125 female rats (weights = 200-250 g) that had been mated for the first time. The test substance was administered orally to three groups of 25 rats in doses of 10, 30, and 90 mg/kg/day, respectively, on gestation days 5 to 16. The doses were administered once daily at a dose volu...","page":25,"pdf":"PRS62.pdf","row_type":"noael_study","study_id":"PRS62_noael_002"}
CIR_vision_codex NOAEL =134 mg/kg/day rat oral 2-week repeated dose toxicity {"citation":"250; 500; (3","dose":"ethal dose in a group of six rabbits was in the range of 250 mg/kg to 500 mg/kg.","effect":"ethal dose in a group of six rabbits was in the range of 250 mg/kg to 500 mg/kg. Minimal nephrosis was the only pathologic change noted in six rats dosed orally with m-Phenylenediamine (3% suspension in peanut oil; dose = 90 mg/kg/day) over a 2-week period. There were not test sub- stance-related pathologic changes in six rats dosed (intragastric intu- bation) with 0.8% m-Phenylenediamine (in mixture; 134 mg/kg/day) over a 2-week period. In a subchronic (90-day) oral toxicity study involving groups of 20 rats, the no-effect level was 6 mg m-Phenylenediamine/kg body weight. At histopathologic examination, degenerative lesions in the liver were observed only in the 18-mg/kg/day dose group. There was no indication of toxic injury to the kidneys.","page":48,"pdf":"PRS62.pdf","row_type":"noael_study","study_id":"PRS62_noael_003"}
EPA_IRIS_iris_rfd_systems.csv 2 endpoints
Source Endpoint Type Value Unit Species Route Duration Study Type Reference
EPA_IRIS_iris_rfd_systems.csv NOEL =6 mg/kg/day - oral chronic IRIS chronic oral RfD system PoD row_hash=bfcae381f66e6e79; file=iris_rfd_systems.csv; kind=point_of_departure; raw_column=point_of_departure; raw_value=NOEL : 6.0 mg/kg-day; system=Hepatic; basis=Increased relative and absolute liver weights and degenerative liver lesions; point_of_departure=NOEL : 6.0 mg/kg-day; composite_uf=1000; confidence=Low; dtxsid=DTXSID4021137; detail_url=https://iris.epa.gov/ChemicalLanding/&substance_nmbr=87; rfd_last_updated=01/31/1987; rfd_pdf_url=https://iris.epa.gov/static/pdfs/0087_summary.pdf
EPA_IRIS_iris_rfd_systems.csv RfD =0.006 mg/kg/day - oral chronic IRIS chronic oral RfD system row_hash=991c4dbb3102b104; file=iris_rfd_systems.csv; kind=reference_value; raw_column=rfd_mg_per_kg_day; raw_value=6e-3; system=Hepatic; basis=Increased relative and absolute liver weights and degenerative liver lesions; point_of_departure=NOEL : 6.0 mg/kg-day; composite_uf=1000; confidence=Low; dtxsid=DTXSID4021137; detail_url=https://iris.epa.gov/ChemicalLanding/&substance_nmbr=87; rfd_last_updated=01/31/1987; rfd_pdf_url=https://iris.epa.gov/static/pdfs/0087_summary.pdf
IARC Monographs 3 endpoints
Source Endpoint Type Value Unit Species Route Duration Study Type Reference
IARC Monographs IARC carcinogenicity classification 3 IARC group - - 1987 IARC Monographs {"additional_info":"volume_publication_year=1987","evaluation_year":1987,"source_table":"iarc_classifications","volume":"16, Sup 7"}
IARC Monographs IARC carcinogenicity classification 3 IARC group - - 1987 IARC Monographs {"additional_info":"volume_publication_year=1987","evaluation_year":1987,"source_table":"iarc_classifications","volume":"16, Sup 7"}
IARC Monographs IARC carcinogenicity classification 3 IARC group - - 1987 IARC Monographs {"additional_info":"volume_publication_year=1987","evaluation_year":1987,"source_table":"iarc_classifications","volume":"16, Sup 7"}
NTP_ICE_acute_oral 2 endpoints
Source Endpoint Type Value Unit Species Route Duration Study Type Reference
NTP_ICE_acute_oral LD50 =280 mg/kg bw Rat oral acute Rat Acute Oral Toxicity NLM ChemIDplus TEST (undated); record_id=acute_oral_736; row=6983; data_type=In Vivo; mixture=Chemical; chemical_name=1,3-Benzenediamine; preferred_name=1,3-Benzenediamine; dtxsid=DTXSID4021137; url=https://chem.nlm.nih.gov/chemidplus/; url_comptox=https://comptox.epa.gov/dashboard/chemical/details/DTXSID4021137; url_cebs=https://doi.org/10.22427/NTP-DATA-DTXSID4021137; source_file=acute_oral.xlsx
NTP_ICE_acute_oral LD50 =650 mg/kg bw Rat oral acute Rat Acute Oral Toxicity NLM Hazardous Substances Data Bank (undated); record_id=acute_oral_737; row=6984; data_type=In Vivo; mixture=Chemical; chemical_name=1,3-Benzenediamine; preferred_name=1,3-Benzenediamine; dtxsid=DTXSID4021137; url=https://pubchem.ncbi.nlm.nih.gov/; url_comptox=https://comptox.epa.gov/dashboard/chemical/details/DTXSID4021137; url_cebs=https://doi.org/10.22427/NTP-DATA-DTXSID4021137; source_file=acute_oral.xlsx
NTP_ICE_adme_parameters 1 endpoint
Source Endpoint Type Value Unit Species Route Duration Study Type Reference
NTP_ICE_adme_parameters Clint 0 uL/min/10^6 cells Human - - Measured; httk, Human Hepatic Intrinsic Clearance sheet=Data; excel_row=1584; Record_ID=adme_parameters_806; Data_Type=Measured; DTXSID=DTXSID4021137; Assay=httk, Human Hepatic Intrinsic Clearance; Endpoint=Clint; Response=0.0; Response_Unit=ul/min/10^6 cells; Species=Human; Reference=httk2.3.1, Wambaugh 2019; URL=https://cran.r-project.org/web/packages/httk/index.html; URL_CompTox=https://comptox.epa.gov/dashboard/chemical/details/DTXSID4021137; URL_CEBS=https://doi.org/10.22427/NTP-DATA-DTXSID4021137
NTP_ICE_cancer 1 endpoint
Source Endpoint Type Value Unit Species Route Duration Study Type Reference
NTP_ICE_cancer IARC group 3 unitless - - - WOE; IARC Carcinogenicity sheet=Data; excel_row=4565; Record_ID=cancer_4704; Data_Type=WOE; Formulation_Name=1,3-Benzenediamine; Mixture=Chemical; DTXSID=DTXSID4021137; Assay=IARC Carcinogenicity; Endpoint=IARC group; Response=3; Response_Unit=Unitless; URL=http://publications.iarc.fr/34; http://publications.iarc.fr/139; URL_CompTox=https://comptox.epa.gov/dashboard/chemical/details/DTXSID4021137; URL_CEBS=https://doi.org/10.22427/NTP-DATA-DTXSID4021137
NTP_ICE_endocrine 1 endpoint
Source Endpoint Type Value Unit Species Route Duration Study Type Reference
NTP_ICE_endocrine Model Score 0 unitless - - - ARPathway2016; AR Pathway Model, Antagonist sheet=Integrated_approaches; excel_row=628; RecordID=ARPathway2016_511; DatasetName=ARPathway2016; DTXSID=DTXSID4021137; Assay=AR Pathway Model, Antagonist; Endpoint=Model Score; Response=0; Response_Unit=Unitless; URL_CompTox=https://comptox.epa.gov/dashboard/chemical/details/DTXSID4021137; URL_CEBS=https://doi.org/10.22427/NTP-DATA-DTXSID4021137
NTP_ICE_eye_irritation 4 endpoints
Source Endpoint Type Value Unit Species Route Duration Study Type Reference
NTP_ICE_eye_irritation GHS Classification 1 unitless Rabbit Ocular - In Vivo; Draize Eye Irritation/Corrosion Test sheet=Data; excel_row=1187; Record_ID=eye_irritation_218; Data_Type=In Vivo; Mixture=Chemical; DTXSID=DTXSID4021137; Assay=Draize Eye Irritation/Corrosion Test; Endpoint=GHS Classification; Response=1; Response_Unit=Unitless; Species=Rabbit; PMID=26472347.0; Reference=Yamaguchi et al. 2016; URL=10.1002/jat.3254; URL_CompTox=https://comptox.epa.gov/dashboard/chemical/details/DTXSID4021137; URL_CEBS=https://doi.org/10.22427/NTP-DATA-DTXSID4021137
NTP_ICE_eye_irritation Intensity 0.35 %/sec - Ocular - In Vitro; Vitrigel sheet=Data; excel_row=1189; Record_ID=eye_irritation_1324; Data_Type=In Vitro; Mixture=Chemical; DTXSID=DTXSID4021137; Assay=Vitrigel; Endpoint=Intensity; Response=0.35; Response_Unit=%/sec; PMID=26472347.0; Reference=Yamaguchi et al. 2016; URL=10.1002/jat.3254; URL_CompTox=https://comptox.epa.gov/dashboard/chemical/details/DTXSID4021137; URL_CEBS=https://doi.org/10.22427/NTP-DATA-DTXSID4021137
NTP_ICE_eye_irritation Lag time 10 s - Ocular - In Vitro; Vitrigel sheet=Data; excel_row=1188; Record_ID=eye_irritation_1324; Data_Type=In Vitro; Mixture=Chemical; DTXSID=DTXSID4021137; Assay=Vitrigel; Endpoint=Lag time; Response=10; Response_Unit=sec; PMID=26472347.0; Reference=Yamaguchi et al. 2016; URL=10.1002/jat.3254; URL_CompTox=https://comptox.epa.gov/dashboard/chemical/details/DTXSID4021137; URL_CEBS=https://doi.org/10.22427/NTP-DATA-DTXSID4021137
NTP_ICE_eye_irritation Plateau level 62 % - Ocular - In Vitro; Vitrigel sheet=Data; excel_row=1190; Record_ID=eye_irritation_1324; Data_Type=In Vitro; Mixture=Chemical; DTXSID=DTXSID4021137; Assay=Vitrigel; Endpoint=Plateau level; Response=62; Response_Unit=%; PMID=26472347.0; Reference=Yamaguchi et al. 2016; URL=10.1002/jat.3254; URL_CompTox=https://comptox.epa.gov/dashboard/chemical/details/DTXSID4021137; URL_CEBS=https://doi.org/10.22427/NTP-DATA-DTXSID4021137
NTP_ICE_skin_sensitization 4 endpoints
Source Endpoint Type Value Unit Species Route Duration Study Type Reference
NTP_ICE_skin_sensitization EC3 0.49 % Mouse Dermal - In Vivo; LLNAdb2013; LLNA sheet=Data_invivo; excel_row=13546; Record_ID=skin_sensitization_invivo_3754; Data_Type=In Vivo; Internal_Data_Source=LLNAdb2013; Mixture=Chemical; DTXSID=DTXSID4021137; Assay=LLNA; Endpoint=EC3; Response=0.49; Response_Unit=%; Species=Mouse; Route=Dermal; Reference=Gerberick et al. 2005; 16536334; Not available; URL_CompTox=https://comptox.epa.gov/dashboard/chemical/details/DTXSID4021137; URL_CEBS=https://doi.org/10.22427/NTP-DATA-DTXSID4021137
NTP_ICE_skin_sensitization EC3 0.49 % Mouse Dermal - In Vivo; LLNAdb2013; LLNA sheet=Data_invivo; excel_row=13546; Record_ID=skin_sensitization_invivo_3754; Data_Type=In Vivo; Internal_Data_Source=LLNAdb2013; Mixture=Chemical; DTXSID=DTXSID4021137; Assay=LLNA; Endpoint=EC3; Response=0.49; Response_Unit=%; Species=Mouse; Route=Dermal; Reference=Gerberick et al. 2005; 16536334; Not available; URL_CompTox=https://comptox.epa.gov/dashboard/chemical/details/DTXSID4021137; URL_CEBS=https://doi.org/10.22427/NTP-DATA-DTXSID4021137
NTP_ICE_skin_sensitization EC3 0.49 % Mouse Dermal - In Vivo; LLNAdb2013; LLNA sheet=Data_invivo; excel_row=13546; Record_ID=skin_sensitization_invivo_3754; Data_Type=In Vivo; Internal_Data_Source=LLNAdb2013; Mixture=Chemical; DTXSID=DTXSID4021137; Assay=LLNA; Endpoint=EC3; Response=0.49; Response_Unit=%; Species=Mouse; Route=Dermal; Reference=Gerberick et al. 2005; 16536334; Not available; URL_CompTox=https://comptox.epa.gov/dashboard/chemical/details/DTXSID4021137; URL_CEBS=https://doi.org/10.22427/NTP-DATA-DTXSID4021137
NTP_ICE_skin_sensitization EC3 0.49 % Mouse Dermal - In Vivo; LLNAdb2013; LLNA sheet=Data_invivo; excel_row=13546; Record_ID=skin_sensitization_invivo_3754; Data_Type=In Vivo; Internal_Data_Source=LLNAdb2013; Mixture=Chemical; DTXSID=DTXSID4021137; Assay=LLNA; Endpoint=EC3; Response=0.49; Response_Unit=%; Species=Mouse; Route=Dermal; Reference=Gerberick et al. 2005; 16536334; Not available; URL_CompTox=https://comptox.epa.gov/dashboard/chemical/details/DTXSID4021137; URL_CEBS=https://doi.org/10.22427/NTP-DATA-DTXSID4021137
ToxValDB_ECHA_IUCLID 18 endpoints
Source Endpoint Type Value Unit Species Route Duration Study Type Reference
ToxValDB_ECHA_IUCLID LEL =720 mg/m3 Rat inhalation - acute QUALITY=2 (reliable with restrictions); STORED_SOURCE_RECORD=https://clowder.edap-cluster.com/files/66059759e4b063812d6fa6de; RECORD_SOURCE_LEVEL=Extraction document; SOURCE_URL=https://echa.europa.eu/; SUBSOURCE_URL=https://echa.europa.eu/registration-dossier/-/registered-dossier/24112/7/3/3?documentUUID=2c44e6c1-a585-4f9e-8cec-c2b81d39768b; YEAR=1988; ORIGINAL_YEAR=1988; STUDY_GROUP=ECHA IUCLID_dup_Acute Toxicity Inhalation_15799165_15799166:M:--; QC_CATEGORY=Programmatically extracted from structured data source; Source overall passed QC, but this record was not manually checked; QC_STATUS=not determined; SOURCE_HASH=ToxValhc_6539c6ee33c5de22efe17e843f50d1f6
ToxValDB_ECHA_IUCLID LEL =1000 mg/kg bw/day Rat oral - acute QUALITY=2 (reliable with restrictions); STORED_SOURCE_RECORD=https://clowder.edap-cluster.com/files/67c61bb0e4b096bca876f187; RECORD_SOURCE_LEVEL=Extraction document; SOURCE_URL=https://echa.europa.eu/; SUBSOURCE_URL=https://echa.europa.eu/registration-dossier/-/registered-dossier/24112/7/3/2?documentUUID=2c44e6c1-a585-4f9e-8cec-c2b81d39768b; YEAR=1988; ORIGINAL_YEAR=1988; STUDY_GROUP=ECHA IUCLID_dup_Acute Toxicity Oral_15799724_15801029_15805452:M:--; QC_CATEGORY=Programmatically extracted from structured data source; Source overall passed QC, but this record was not manually checked; QC_STATUS=not determined; SOURCE_HASH=ToxValhc_7596e54c928d1dfe36be148df33911d3
ToxValDB_ECHA_IUCLID LEL =450 mg/kg bw/day Rat oral - acute QUALITY=2 (reliable with restrictions); STORED_SOURCE_RECORD=https://clowder.edap-cluster.com/files/6605975fe4b063812d6fa6ed; RECORD_SOURCE_LEVEL=Extraction document; SOURCE_URL=https://echa.europa.eu/; SUBSOURCE_URL=https://echa.europa.eu/registration-dossier/-/registered-dossier/24112/7/3/2?documentUUID=2c44e6c1-a585-4f9e-8cec-c2b81d39768b; YEAR=1988; ORIGINAL_YEAR=1988; STUDY_GROUP=ECHA IUCLID_dup_Acute Toxicity Oral_15799724_15801029_15805452:M:--; QC_CATEGORY=Programmatically extracted from structured data source; Source overall passed QC, but this record was not manually checked; QC_STATUS=not determined; SOURCE_HASH=ToxValhc_e1bbf396d54ad6ec198950810467ca7a
ToxValDB_ECHA_IUCLID LEL =25 mg/kg bw/day Cat oral - acute QUALITY=4 (not assignable); STORED_SOURCE_RECORD=https://clowder.edap-cluster.com/files/6605975fe4b063812d6fa6ed; RECORD_SOURCE_LEVEL=Extraction document; SOURCE_URL=https://echa.europa.eu/; SUBSOURCE_URL=https://echa.europa.eu/registration-dossier/-/registered-dossier/24112/7/3/2?documentUUID=2c44e6c1-a585-4f9e-8cec-c2b81d39768b; YEAR=1988; ORIGINAL_YEAR=1988; STUDY_GROUP=ECHA IUCLID:15812401:-:--; QC_CATEGORY=Programmatically extracted from structured data source; Source overall passed QC, but this record was not manually checked; QC_STATUS=not determined; SOURCE_HASH=ToxValhc_8827c155942f37a3b5f84ed3a3ab8ba2
ToxValDB_ECHA_IUCLID LEL =400 mg/kg bw/day Mouse injection - acute QUALITY=4 (not assignable); STORED_SOURCE_RECORD=https://clowder.edap-cluster.com/files/67c61bf1e4b096bca8770079; RECORD_SOURCE_LEVEL=Extraction document; SOURCE_URL=https://echa.europa.eu/; SUBSOURCE_URL=https://echa.europa.eu/registration-dossier/-/registered-dossier/24112/7/3/5?documentUUID=2c44e6c1-a585-4f9e-8cec-c2b81d39768b; YEAR=1988; ORIGINAL_YEAR=1988; STUDY_GROUP=ECHA IUCLID:15815110:-:--; QC_CATEGORY=Programmatically extracted from structured data source; Source overall passed QC, but this record was not manually checked; QC_STATUS=not determined; SOURCE_HASH=ToxValhc_fd5b5db047af25bd69c06185419a72c9
ToxValDB_ECHA_IUCLID LEL =370 mg/kg bw/day Rabbit injection - acute QUALITY=4 (not assignable); STORED_SOURCE_RECORD=https://clowder.edap-cluster.com/files/67c61c45e4b096bca877148b; RECORD_SOURCE_LEVEL=Extraction document; SOURCE_URL=https://echa.europa.eu/; SUBSOURCE_URL=https://echa.europa.eu/registration-dossier/-/registered-dossier/24112/7/3/5?documentUUID=2c44e6c1-a585-4f9e-8cec-c2b81d39768b; YEAR=1988; ORIGINAL_YEAR=1988; STUDY_GROUP=ECHA IUCLID_dup_Acute Toxicity Other Routes_15815317_15816037_15816038:-:--; QC_CATEGORY=Programmatically extracted from structured data source; Source overall passed QC, but this record was not manually checked; QC_STATUS=not determined; SOURCE_HASH=ToxValhc_6b96791b88ae985d47d54ec4e1379597
ToxValDB_ECHA_IUCLID LEL =460 mg/kg bw/day Rat injection - acute QUALITY=4 (not assignable); STORED_SOURCE_RECORD=https://clowder.edap-cluster.com/files/67c61c89e4b096bca8772637; RECORD_SOURCE_LEVEL=Extraction document; SOURCE_URL=https://echa.europa.eu/; SUBSOURCE_URL=https://echa.europa.eu/registration-dossier/-/registered-dossier/24112/7/3/5?documentUUID=2c44e6c1-a585-4f9e-8cec-c2b81d39768b; YEAR=1988; ORIGINAL_YEAR=1988; STUDY_GROUP=ECHA IUCLID:15815510:-:--; QC_CATEGORY=Programmatically extracted from structured data source; Source overall passed QC, but this record was not manually checked; QC_STATUS=not determined; SOURCE_HASH=ToxValhc_996b0d81ab1b44b0291a3b627bee8ef5
ToxValDB_ECHA_IUCLID LEL >=200 mg/kg bw/day Cat injection - acute QUALITY=4 (not assignable); STORED_SOURCE_RECORD=https://clowder.edap-cluster.com/files/67c61d0de4b096bca87747e2; RECORD_SOURCE_LEVEL=Extraction document; SOURCE_URL=https://echa.europa.eu/; SUBSOURCE_URL=https://echa.europa.eu/registration-dossier/-/registered-dossier/24112/7/3/5?documentUUID=2c44e6c1-a585-4f9e-8cec-c2b81d39768b; YEAR=1988; ORIGINAL_YEAR=1988; STUDY_GROUP=ECHA IUCLID_dup_Acute Toxicity Other Routes_15816031_15816032:-:--; QC_CATEGORY=Programmatically extracted from structured data source; Source overall passed QC, but this record was not manually checked; QC_STATUS=not determined; SOURCE_HASH=ToxValhc_324bdf3407dcb906b15e364eaa522af2
ToxValDB_ECHA_IUCLID LEL <=435 mg/kg bw/day Cat injection - acute QUALITY=4 (not assignable); STORED_SOURCE_RECORD=https://clowder.edap-cluster.com/files/67c61d0de4b096bca87747e2; RECORD_SOURCE_LEVEL=Extraction document; SOURCE_URL=https://echa.europa.eu/; SUBSOURCE_URL=https://echa.europa.eu/registration-dossier/-/registered-dossier/24112/7/3/5?documentUUID=2c44e6c1-a585-4f9e-8cec-c2b81d39768b; YEAR=1988; ORIGINAL_YEAR=1988; STUDY_GROUP=ECHA IUCLID_dup_Acute Toxicity Other Routes_15816031_15816032:-:--; QC_CATEGORY=Programmatically extracted from structured data source; Source overall passed QC, but this record was not manually checked; QC_STATUS=not determined; SOURCE_HASH=ToxValhc_262e5d09b7648a2856a703f2d3d70979
ToxValDB_ECHA_IUCLID LEL <=440 mg/kg bw/day Rabbit injection - acute QUALITY=4 (not assignable); STORED_SOURCE_RECORD=https://clowder.edap-cluster.com/files/67c61d2ae4b096bca8774e00; RECORD_SOURCE_LEVEL=Extraction document; SOURCE_URL=https://echa.europa.eu/; SUBSOURCE_URL=https://echa.europa.eu/registration-dossier/-/registered-dossier/24112/7/3/5?documentUUID=2c44e6c1-a585-4f9e-8cec-c2b81d39768b; YEAR=1988; ORIGINAL_YEAR=1988; STUDY_GROUP=ECHA IUCLID_dup_Acute Toxicity Other Routes_15815317_15816037_15816038:-:--; QC_CATEGORY=Programmatically extracted from structured data source; Source overall passed QC, but this record was not manually checked; QC_STATUS=not determined; SOURCE_HASH=ToxValhc_62f305c170e65247ffc001d294c6332a
ToxValDB_ECHA_IUCLID LEL >100 mg/kg bw/day Rat oral short-term; 4 weeks short-term QUALITY=2 (reliable with restrictions); STORED_SOURCE_RECORD=https://clowder.edap-cluster.com/files/669eaccce4b0a7c65d1c0e4d; RECORD_SOURCE_LEVEL=Extraction document; SOURCE_URL=https://echa.europa.eu/; SUBSOURCE_URL=https://echa.europa.eu/registration-dossier/-/registered-dossier/24112/7/6/2?documentUUID=2c44e6c1-a585-4f9e-8cec-c2b81d39768b; YEAR=1988; ORIGINAL_YEAR=1988; STUDY_GROUP=ECHA IUCLID:15831863:M/F:--; QC_CATEGORY=Programmatically extracted from structured data source; Source overall passed QC, but this record was not manually checked; QC_STATUS=not determined; SOURCE_HASH=ToxValhc_0c0f4ea26b8be33751e092107096ceca
ToxValDB_ECHA_IUCLID NOAEL =38.2 mg/kg bw/day Mouse oral - chronic QUALITY=2 (reliable with restrictions); STORED_SOURCE_RECORD=https://clowder.edap-cluster.com/files/669ea9cee4b0a7c65d1b2ce8; RECORD_SOURCE_LEVEL=Extraction document; SOURCE_URL=https://echa.europa.eu/; SUBSOURCE_URL=https://echa.europa.eu/registration-dossier/-/registered-dossier/24112/7/8?documentUUID=2c44e6c1-a585-4f9e-8cec-c2b81d39768b; YEAR=1988; ORIGINAL_YEAR=1988; STUDY_GROUP=ECHA IUCLID:15819543:M:--; QC_CATEGORY=Programmatically extracted from structured data source; Source overall passed QC, but this record was not manually checked; QC_STATUS=not determined; SOURCE_HASH=ToxValhc_a44b7db88ee525151117f319b2a1a17d
ToxValDB_ECHA_IUCLID NOAEL =41.8 mg/kg bw/day Mouse oral - chronic QUALITY=2 (reliable with restrictions); STORED_SOURCE_RECORD=https://clowder.edap-cluster.com/files/669ea9cee4b0a7c65d1b2ce8; RECORD_SOURCE_LEVEL=Extraction document; SOURCE_URL=https://echa.europa.eu/; SUBSOURCE_URL=https://echa.europa.eu/registration-dossier/-/registered-dossier/24112/7/8?documentUUID=2c44e6c1-a585-4f9e-8cec-c2b81d39768b; YEAR=1988; ORIGINAL_YEAR=1988; STUDY_GROUP=ECHA IUCLID:15819544:F:--; QC_CATEGORY=Programmatically extracted from structured data source; Source overall passed QC, but this record was not manually checked; QC_STATUS=not determined; SOURCE_HASH=ToxValhc_656189ddde8f3b034ab36ff1ec9608a8
ToxValDB_ECHA_IUCLID NOAEL =30 mg/kg bw/day Rat oral - developmental QUALITY=2 (reliable with restrictions); STORED_SOURCE_RECORD=https://clowder.edap-cluster.com/files/669eabb9e4b0a7c65d1bb707; RECORD_SOURCE_LEVEL=Extraction document; SOURCE_URL=https://echa.europa.eu/; SUBSOURCE_URL=https://echa.europa.eu/registration-dossier/-/registered-dossier/24112/7/9/3?documentUUID=2c44e6c1-a585-4f9e-8cec-c2b81d39768b; YEAR=1988; ORIGINAL_YEAR=1988; STUDY_GROUP=ECHA IUCLID:15821078:-:-fetal; QC_CATEGORY=Programmatically extracted from structured data source; Source overall passed QC, but this record was not manually checked; QC_STATUS=not determined; SOURCE_HASH=ToxValhc_253f32af249f3404a1a60f3b611461bd
ToxValDB_ECHA_IUCLID NOAEL =20 mg/kg bw/day Rat oral - repeat dose other GUIDELINE=EPA OTS 798.6050 (Neurotoxicity Screening Battery); QUALITY=1 (reliable without restriction); STORED_SOURCE_RECORD=https://clowder.edap-cluster.com/files/66a7c85ae4b0a7c65d2180e9; RECORD_SOURCE_LEVEL=Extraction document; SOURCE_URL=https://echa.europa.eu/; SUBSOURCE_URL=https://echa.europa.eu/registration-dossier/-/registered-dossier/24112/7/10/1?documentUUID=2c44e6c1-a585-4f9e-8cec-c2b81d39768b; YEAR=1988; ORIGINAL_YEAR=1988; STUDY_GROUP=ECHA IUCLID_dup_Neurotoxicity_15825726_15825727_15825796:M/F:--; QC_CATEGORY=Programmatically extracted from structured data source; Source overall passed QC, but this record was not manually checked; QC_STATUS=not determined; SOURCE_HASH=ToxValhc_f3d104ac276b1cb3907a4f8772eaf037
ToxValDB_ECHA_IUCLID NOAEL >=300 mg/kg bw/day Rat oral - repeat dose other QUALITY=2 (reliable with restrictions); STORED_SOURCE_RECORD=https://clowder.edap-cluster.com/files/669eaa3ee4b0a7c65d1b4ec5; RECORD_SOURCE_LEVEL=Extraction document; SOURCE_URL=https://echa.europa.eu/; SUBSOURCE_URL=https://echa.europa.eu/registration-dossier/-/registered-dossier/24112/7/10/1?documentUUID=2c44e6c1-a585-4f9e-8cec-c2b81d39768b; YEAR=1988; ORIGINAL_YEAR=1988; STUDY_GROUP=ECHA IUCLID_dup_Neurotoxicity_15825726_15825727_15825796:M/F:--; QC_CATEGORY=Programmatically extracted from structured data source; Source overall passed QC, but this record was not manually checked; QC_STATUS=not determined; SOURCE_HASH=ToxValhc_78199babda421d27ade45cc18a10699d
ToxValDB_ECHA_IUCLID NOAEL =6 mg/kg bw/day Rat oral subchronic; 13 weeks subchronic QUALITY=2 (reliable with restrictions); STORED_SOURCE_RECORD=https://clowder.edap-cluster.com/files/669eaccce4b0a7c65d1c0e4f; RECORD_SOURCE_LEVEL=Extraction document; SOURCE_URL=https://echa.europa.eu/; SUBSOURCE_URL=https://echa.europa.eu/registration-dossier/-/registered-dossier/24112/7/6/2?documentUUID=2c44e6c1-a585-4f9e-8cec-c2b81d39768b; YEAR=1988; ORIGINAL_YEAR=1988; STUDY_GROUP=ECHA IUCLID:15846192:M/F:--; QC_CATEGORY=Programmatically extracted from structured data source; Source overall passed QC, but this record was not manually checked; QC_STATUS=not determined; SOURCE_HASH=ToxValhc_b48c7ed7ee2ea074c7ad4fbf3889f0de
ToxValDB_ECHA_IUCLID NOEL =5 mg/kg bw/day Rat oral - repeat dose other GUIDELINE=EPA OTS 798.6050 (Neurotoxicity Screening Battery); QUALITY=1 (reliable without restriction); STORED_SOURCE_RECORD=https://clowder.edap-cluster.com/files/66a7c85ae4b0a7c65d2180e9; RECORD_SOURCE_LEVEL=Extraction document; SOURCE_URL=https://echa.europa.eu/; SUBSOURCE_URL=https://echa.europa.eu/registration-dossier/-/registered-dossier/24112/7/10/1?documentUUID=2c44e6c1-a585-4f9e-8cec-c2b81d39768b; YEAR=1988; ORIGINAL_YEAR=1988; TOXICOLOGICAL_EFFECT=body weight and weight gain|clinical signs|food efficiency; TOXICOLOGICAL_EFFECT_CATEGORY=body weight|clinical signs|other; STUDY_GROUP=ECHA IUCLID_dup_Neurotoxicity_15825726_15825727_15825796:M/F:--; QC_CATEGORY=Programmatically extracted from structured data source; Source overall passed QC, but this record was not manually checked; QC_STATUS=not determined; SOURCE_HASH=ToxValhc_fc5a9178233e18e718162b08cfb6d5d8
ToxValDB_GESTIS_DNEL 1 endpoint
Source Endpoint Type Value Unit Species Route Duration Study Type Reference
ToxValDB_GESTIS_DNEL DNEL systemic =0.24 mg/m3 Human inhalation - Toxicity Value STORED_SOURCE_RECORD=https://clowder.edap-cluster.com/files/6543dd69e4b045b9ff7cd87e; RECORD_SOURCE_LEVEL=Extraction document; SOURCE_URL=https://www.dguv.de/ifa/gestis/gestis-dnel-liste/index-2.jsp; STUDY_GROUP=GESTIS DNEL:15634098:-:--; QC_CATEGORY=Programmatically extracted from structured data source; Source overall passed QC, but this record was not manually checked; QC_STATUS=not determined; SOURCE_HASH=ToxValhc_978e764e922bebdc2f1f25dd566abf3a
ToxValDB_IRIS 2 endpoints
Source Endpoint Type Value Unit Species Route Duration Study Type Reference
ToxValDB_IRIS LOAEL =18 mg/kg bw/day Rat oral subchronic; 90 days subchronic LONG_REF=Hofer, H., R. Hruby, E Hruby, et al. 1982. Ninety-day toxicity study with m- phenylenediamine on rats. Oestrr. Forschungszent. Seibersdorf (Ber.) OEFZS Ber. No. 4155. p. 1-46.; TITLE=p; AUTHOR=Hofer, H., R. Hruby, E Hruby, et al; STORED_SOURCE_RECORD=https://clowder.edap-cluster.com/files/652e8a2ce4b045b9ff7a4d5e; RECORD_SOURCE_LEVEL=Extraction document; SOURCE_URL=https://www.epa.gov/iris; SUBSOURCE_URL=https://iris.epa.gov/ChemicalLanding/&substance_nmbr=87; TOXICOLOGICAL_EFFECT=increased relative and absolute liver weight and degenerative liver lesions; TOXICOLOGICAL_EFFECT_CATEGORY=multiple; STUDY_GROUP=IRIS_dup_IRIS Summary_15645393_15645394:M/F:--; QC_CATEGORY=Manually extracted from unstructured data source; Source overall passed QC, and this record was manually checked; QC_STATUS=pass; SOURCE_HASH=ToxValhc_57e1dffbe556b4a3fe38ac40762b8842
ToxValDB_IRIS RfD =0.006 mg/kg bw/day Human oral - Toxicity Value LONG_REF=Hofer, H., R. Hruby, E Hruby, et al. 1982. Ninety-day toxicity study with m- phenylenediamine on rats. Oestrr. Forschungszent. Seibersdorf (Ber.) OEFZS Ber. No. 4155. p. 1-46.; TITLE=p; AUTHOR=Hofer, H., R. Hruby, E Hruby, et al; STORED_SOURCE_RECORD=https://clowder.edap-cluster.com/files/652e8a2ce4b045b9ff7a4d5e; RECORD_SOURCE_LEVEL=Extraction document; SOURCE_URL=https://www.epa.gov/iris; SUBSOURCE_URL=https://iris.epa.gov/ChemicalLanding/&substance_nmbr=87; TOXICOLOGICAL_EFFECT=Increased relative and absolute liver weights and degenerative liver lesions in male/female rats; STUDY_GROUP=IRIS:15645141:-:--; QC_CATEGORY=Manually extracted from unstructured data source; Source overall passed QC, and this record was manually checked; QC_STATUS=pass; SOURCE_HASH=ToxValhc_4c40d7c3351d53557765d5616655c21f
ToxValDB_RSL 1 endpoint
Source Endpoint Type Value Unit Species Route Duration Study Type Reference
ToxValDB_RSL RfD =0.06 mg/kg bw/day Human oral - Toxicity Value STORED_SOURCE_RECORD=https://clowder.edap-cluster.com/files/6759b87ce4b0a7c65d37b4e2; RECORD_SOURCE_LEVEL=Extraction document; SOURCE_URL=https://www.epa.gov/risk/regional-screening-levels-rsls-generic-tables; STUDY_GROUP=RSL:15663670:-:--; QC_CATEGORY=Programmatically extracted from structured data source; Source overall passed QC, but this record was not manually checked; QC_STATUS=not determined; SOURCE_HASH=ToxValhc_365ac5accfd4553e3ca2ca1ff8456aa1
UnifiedCodex:CIR:beta.noael_studies 3 endpoints
Source Endpoint Type Value Unit Species Route Duration Study Type Reference
UnifiedCodex:CIR:beta.noael_studies developmental toxicity 5 mg/kg rat - - developmental toxicity SOURCE_SUBDIR=PRS62; REPORT_TITLE=FINAL REPORT ON THE SAFETY ASSESSMENT OF m-PHENYLENEDIAMINE AND m-PHENYLENEDIAMINE SULFATE; OPINION_NUMBER=PRS62; COMMITTEE=Cosmetic Ingredient Review Expert Panel; REPORT_DATE=1101; VALUE_TEXT=5; DOSE=It was concluded that m-Phenylenediamine was not neurotoxic and that the no observable effect level for this chemical in male and female rats was 5 mg/kg (Du Pont, 1992).; EFFECT=ons were not considered neurotoxic effects but were considered indicative of general malaise in experimental animals. The general malaise was supported by concurrent clinical observations of lethargy. In female rats, the test substance did not induce changes in horizontal or vertical motor activity counts at any of the doses tested. Neuropathologic exam- inations did not indicate any abnormalities within the nervous system or skeletal muscle. It was concluded that m-Phenylenediamine was not neurotoxic and that the no observable effect level for this chemical in male and female rats was 5 mg/kg (Du Pont, 1992). Reproductive Toxicity The results of six reproductive toxicity studies are summarized in Table 7. In the first study, the fetal toxicity of m-Phenylenediamine (99% pure) in water was evaluated using 125 female rats (weights = 200-250 g) that had been mated for the first time. The test substance was administered orally to three groups of 25 rats in doses of 10, 30, and 90 mg/kg/day, respectively, on gestation days 5 to 16. The doses were administered once daily at a dose volu...; CITATION=5; 7; (99; CITATION_NUMBERS=[5,7,99]; REFERENCE=5; 7; (99; DETAILS_JSON={"cas_number":"108-45-2","citation":"5; 7; (99","dose":"It was concluded that m-Phenylenediamine was not neurotoxic and that the no observable effect level for this chemical in male and female rats was 5 mg/kg (Du Pont, 1992).","duration":"","effect":"ons were not considered neurotoxic effects but were considered indicative of general malaise in experimental animals. The general malaise was supported by concurrent clinical observations of lethargy. In female rats, the test substance did not induce changes in horizontal or vertical motor activity counts at any of the doses tested. Neuropathologic exam- inations did not indicate any abnormalities within the nervous system or skeletal muscle. It was concluded that m-Phenylenediamine was not neurotoxic and that the no observable effect level for this chemical in male and female rats was 5 mg/kg (Du Pont, 1992). Reproductive Toxicity The results of six reproductive toxicity studies are summarized in Table 7. In the first study, the fetal toxicity of m-Phenylenediamine (99% pure) in water was evaluated using 125 female rats (weights = 200-250 g) that had been mated for the first time. The test substance was administered orally to three groups of 25 rats in doses of 10, 30, and 90 mg/kg/day, respectively, on gestation days 5 to 16. The doses were administered once daily at a dose volu...","endpoint":"developmental toxicity","ingredient":"THE SAFETY ASSESSMENT OF m-PHENYLENEDIAMINE AND m-PHENYLENEDIAMINE SULFATE","loael_value":"","noael_unit":"mg/kg","noael_value":"5","page":25,"route":"","species":"rat","study_id":"PRS62_noael_002"}
UnifiedCodex:CIR:beta.noael_studies repeated dose toxicity 6 mg/kg rat dermal Subchronic repeated dose toxicity SOURCE_SUBDIR=PRS62; REPORT_TITLE=FINAL REPORT ON THE SAFETY ASSESSMENT OF m-PHENYLENEDIAMINE AND m-PHENYLENEDIAMINE SULFATE; OPINION_NUMBER=PRS62; COMMITTEE=Cosmetic Ingredient Review Expert Panel; REPORT_DATE=1101; VALUE_TEXT=6.0; DOSE=Toxic effects were not observed in rats dosed with 2.0 or 6.0 mg/kg m-Phenylenediamine.; EFFECT=test substance-related effect could be made based on necropsy findings in animals that survived to the end of the study. Necropsy results included isolated evidence of various spontaneous alterations, such as congenital fissurations of the spleen and liver nodules or testicular atrophy. Toxic effects were not observed in rats dosed with 2.0 or 6.0 mg/kg m-Phenylenediamine. It was concluded that the highest daily dose that could be administered to a group without cumulative damage and/or substance-related changes (no-effect-level) was 6 mg m- Phenylenediamine/kg body weight. Subchronic Dermal Toxicity The subchronic dermal toxicity of an oxidative dye formulation contain- ing 1.5% m-Phenylenediamine was evaluated using 12 adult New Zealand white rabbits (six males, six females; weights not stated). Three groups of 12 untreated rabbits served as controls. The dye was mixed with an equal volume of 6% hydrogen peroxide and applied (dose = 1 mL/kg) to the dorsolateral aspects of the thoracic-lumbar area (one on each side of the midline). The test sites were alternated in order to minim...; CITATION=2; 0; 6; CITATION_NUMBERS=[2,6]; REFERENCE=2; 0; 6; DETAILS_JSON={"cas_number":"108-45-2","citation":"2; 0; 6","dose":"Toxic effects were not observed in rats dosed with 2.0 or 6.0 mg/kg m-Phenylenediamine.","duration":"Subchronic","effect":"test substance-related effect could be made based on necropsy findings in animals that survived to the end of the study. Necropsy results included isolated evidence of various spontaneous alterations, such as congenital fissurations of the spleen and liver nodules or testicular atrophy. Toxic effects were not observed in rats dosed with 2.0 or 6.0 mg/kg m-Phenylenediamine. It was concluded that the highest daily dose that could be administered to a group without cumulative damage and/or substance-related changes (no-effect-level) was 6 mg m- Phenylenediamine/kg body weight. Subchronic Dermal Toxicity The subchronic dermal toxicity of an oxidative dye formulation contain- ing 1.5% m-Phenylenediamine was evaluated using 12 adult New Zealand white rabbits (six males, six females; weights not stated). Three groups of 12 untreated rabbits served as controls. The dye was mixed with an equal volume of 6% hydrogen peroxide and applied (dose = 1 mL/kg) to the dorsolateral aspects of the thoracic-lumbar area (one on each side of the midline). The test sites were alternated in order to minim...","endpoint":"repeated dose toxicity","ingredient":"THE SAFETY ASSESSMENT OF m-PHENYLENEDIAMINE AND m-PHENYLENEDIAMINE SULFATE","loael_value":"","noael_unit":"mg/kg","noael_value":"6.0","page":18,"route":"dermal","species":"rat","study_id":"PRS62_noael_001"}
UnifiedCodex:CIR:beta.noael_studies repeated dose toxicity 134 mg/kg/day rat oral 2-week repeated dose toxicity SOURCE_SUBDIR=PRS62; REPORT_TITLE=FINAL REPORT ON THE SAFETY ASSESSMENT OF m-PHENYLENEDIAMINE AND m-PHENYLENEDIAMINE SULFATE; OPINION_NUMBER=PRS62; COMMITTEE=Cosmetic Ingredient Review Expert Panel; REPORT_DATE=1101; VALUE_TEXT=134; DOSE=ethal dose in a group of six rabbits was in the range of 250 mg/kg to 500 mg/kg.; EFFECT=ethal dose in a group of six rabbits was in the range of 250 mg/kg to 500 mg/kg. Minimal nephrosis was the only pathologic change noted in six rats dosed orally with m-Phenylenediamine (3% suspension in peanut oil; dose = 90 mg/kg/day) over a 2-week period. There were not test sub- stance-related pathologic changes in six rats dosed (intragastric intu- bation) with 0.8% m-Phenylenediamine (in mixture; 134 mg/kg/day) over a 2-week period. In a subchronic (90-day) oral toxicity study involving groups of 20 rats, the no-effect level was 6 mg m-Phenylenediamine/kg body weight. At histopathologic examination, degenerative lesions in the liver were observed only in the 18-mg/kg/day dose group. There was no indication of toxic injury to the kidneys.; CITATION=250; 500; (3; CITATION_NUMBERS=[250,500,3]; REFERENCE=250; 500; (3; DETAILS_JSON={"cas_number":"108-45-2","citation":"250; 500; (3","dose":"ethal dose in a group of six rabbits was in the range of 250 mg/kg to 500 mg/kg.","duration":"2-week","effect":"ethal dose in a group of six rabbits was in the range of 250 mg/kg to 500 mg/kg. Minimal nephrosis was the only pathologic change noted in six rats dosed orally with m-Phenylenediamine (3% suspension in peanut oil; dose = 90 mg/kg/day) over a 2-week period. There were not test sub- stance-related pathologic changes in six rats dosed (intragastric intu- bation) with 0.8% m-Phenylenediamine (in mixture; 134 mg/kg/day) over a 2-week period. In a subchronic (90-day) oral toxicity study involving groups of 20 rats, the no-effect level was 6 mg m-Phenylenediamine/kg body weight. At histopathologic examination, degenerative lesions in the liver were observed only in the 18-mg/kg/day dose group. There was no indication of toxic injury to the kidneys.","endpoint":"repeated dose toxicity","ingredient":"THE SAFETY ASSESSMENT OF m-PHENYLENEDIAMINE AND m-PHENYLENEDIAMINE SULFATE","loael_value":"","noael_unit":"mg/kg/day","noael_value":"134","page":48,"route":"oral","species":"rat","study_id":"PRS62_noael_003"}
openFDA substances 4 endpoints
Source Endpoint Type Value Unit Species Route Duration Study Type Reference
openFDA substances FDA UNII substance identifier OE624J2447 UNII - - - chemical {"approval_status":null,"molecular_formula":"C6H8N2","source_table":"substance_identifiers_fda","substance_class":"chemical","unii_code":"OE624J2447"}
openFDA substances FDA UNII substance identifier OE624J2447 UNII - - - chemical {"approval_status":null,"molecular_formula":"C6H8N2","source_table":"substance_identifiers_fda","substance_class":"chemical","unii_code":"OE624J2447"}
openFDA substances FDA UNII substance identifier OE624J2447 UNII - - - chemical {"approval_status":null,"molecular_formula":"C6H8N2","source_table":"substance_identifiers_fda","substance_class":"chemical","unii_code":"OE624J2447"}
openFDA substances FDA UNII substance identifier OE624J2447 UNII - - - chemical {"approval_status":null,"molecular_formula":"C6H8N2","source_table":"substance_identifiers_fda","substance_class":"chemical","unii_code":"OE624J2447"}